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Beilstein J. Org. Chem. 2016, 12, 1557–1565, doi:10.3762/bjoc.12.150
Graphical Abstract
Scheme 1: Synthesis of the monomethylpalladium(II) complexes 9–11 (in DCM) and 12 (in CH3CN).
Figure 1: Possible isomers.
Figure 2: ORTEP [39] style plot of complex 9 in the solid state. Thermal ellipsoids are given at the 50% probabil...
Figure 3: ORTEP [39] style plot of complex 12 in the solid state. Thermal ellipsoids are drawn at the 50% probabi...
Scheme 2: Synthesis of complex 13.
Figure 4: ORTEP [39] style plot of complex 13 in the solid state. Thermal ellipsoids are drawn at the 50% probabi...
Scheme 3: Possible pathways of methyl trifluoroacetate formation starting from complex 13.
Scheme 4: Synthesis of complex 14 by conversion of complex 13 with iodobenzene bistrifluoroacetate.
Scheme 5: Synthesis of the [((pym)^(NHC-R))PdII(CH3)2] complex 15.